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Sunday, May 10, 2020 | History

3 edition of Transient techniques in NMR of solids found in the catalog.

Transient techniques in NMR of solids

an introduction to theory and practice

by B. C. Gerstein

  • 191 Want to read
  • 35 Currently reading

Published by Academic Press in Orlando, Fla .
Written in English

    Subjects:
  • Solids -- Spectra.,
  • Nuclear magnetic resonance spectroscopy.

  • Edition Notes

    Other titlesTransient techniques in N.M.R. of solids.
    StatementB.C. Gerstein, C.R. Dybowski.
    ContributionsDybowski, C. R.
    Classifications
    LC ClassificationsQC176.8.O6 G47 1985
    The Physical Object
    Paginationxi, 295 p. :
    Number of Pages295
    ID Numbers
    Open LibraryOL3021071M
    ISBN 100122811801
    LC Control Number85001231

    This book is for those familiar with solution-state NMR who are encountering solid-state NMR for the first time. It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. This dual requirement is met through careful construction of. Understanding NMR Spectroscopy. This note covers the following topics: NMR and energy levels, The vector model, Fourier transformation and data processing, How the spectrometer works, Product operators, Two-Dimensional NMR, Relaxation, Phase cyling and gradient pulses.

    Summary. Solid-state NMR is a powerful physical method widely applied in modern fundamental and applied science, medicine, and industry. Its role is particularly valuable in materials chemistry due to the capability of solid-state NMR to rapidly solve tasks connected with structural descriptions of complex systems on macro and/or molecular levels, and the identification of the dynamics often. The underlying physical principles of the latest NMR methodology for probing solid materials are stressed. Techniques covered include pulse Fourier transform with emphasis on the difficulties of recording broad resonances and strategies for overcoming them. Selective experiments such as polarization transfer are included.

    Chapter 1 INTRODUCTION TO NMR SPECTROSCOPY Introduction Figure Protein struc-ture determined by NMR spectroscopy. Four struc-tures of a residue pro-tein, derived from NMR constraints, are overlaid to highlight the accuracy of structure determination by NMR spectroscopy. Nuclear magnetic resonance (NMR) is a spec-. Basic NMR Concepts: A Guide for the Modern Laboratory Description: This handout is designed to furnish you with a basic understanding of Nuclear Magnetic Resonance (NMR) Spectroscopy. The concepts implicit and fundamental to the operation of a modern NMR spectrometer, with generic illustrations where appropriate, will be described.


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Transient techniques in NMR of solids by B. C. Gerstein Download PDF EPUB FB2

In addition to assisting entrance into the field, Transient Techniques in NMR of Solids will be a useful guide for professionals already working in related areas of chemistry. FROM THE PREFACE: Nuclear magnetic resonance (NMR) is truly a remarkable phenomenon. Cited by: Transient Techniques in NMR of Solids.

An Introduction to Theory and Practice. Von B. Gerstein und C. Dybowski. Academic Press, New York XI, S., geb. $ – ISBN 0‐12‐‐1Author: Ulrich Haeberlen. Title - Transient Techniques in NMR of Solids: An Introduction to Theory and Practice.

Authors - B.C. Gerstein and C.R. Dybowski. ISBN This is an excellent book for the student and the expert in Solid State NMR. Drs.5/5. Book Review: Transient techniques in NMR of solids—an introduction to theory and practice.

Gerstein and C. Dybowski. Academic Press, San Diego, pages, $ Transient techniques in NMR of solids: an introduction to theory and practice / B.

Gerstein, C. Dybowski. Also Titled Transient techniques in N.M.R. of solids. Solid-state NMR covers an enormous range of material types and experimental techniques.

Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques.

Transient techniques in NMR of solids: an introduction to theory and practice, Bernard C. Gerstein and C. Dybowski, Academic Press, Orlando (). Nuclear Magnetic Resonance of Liquid Crystals, J.

Emsley (Ed.), NATO ASI Series C, Mathematical and Physical Sciences - Vol. NATO ASI, San Miniato (). The second part mainly deals with the experimental design of solid-state high-resolution NMR experiments to suppress certain interactions and with wide-line experiments. Finally the principles of NMR imaging and NMR microscopy are described as an alternative method for investigating solids by by: Here we suggest a few methods of 1 H NMR imaging of solids at high resolution with chemical selection.

As with most areas of NMR, there is no “best” experiment in general, and we will attempt to show the flexibility of these methods and how they may be employed for a given sample or by: 6. Specialized solid-state NMR techniques manage and even take advantage of this anisotropy.

Magic Angle Spinning. Many solid-state NMR techniques mimic the free tumbling of molecules in liquids by spinning the sample during data acquisition. Spinning rapidly enough at a specific angle to the baseline magnetic field – the magic angle – can.

New techniques continue to emerge and the application of NMR methods continues to expand. High-Resolution NMR Techniques in Organic Chemistry is designed for use in academic and industrial NMR facilities, as a text for graduate-level NMR courses, and as an accessible reference for the chemist's or spectroscopist's desk.

Additional Physical Format: Online version: Gerstein, B.C. (Bernard C.), Transient techniques in NMR of solids. Orlando, Fla.: Academic Press, • Solids NMR spectra of half-integer-spin quadrupolar nuclei have a moderately broad central transition (kHz) and extremely broad satellite transitions (MHz).

• Solids NMR spectra of integer-spin quadrupolar nuclei have broad satellite transitions (MHz) and no central Size: 6MB. High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most important NMR spectroscopy techniques for the structure elucidation of organic molecules and the investigation of their behaviour in solution.

Appropriate for advanced undergraduate and graduate students, research chemists and NMR facility managers, this thorough revision covers practical aspects of NMR. Deuterium NMR in Solids. This book offers a concise introduction to the angular momentum, one of the most fundamental quantities in all of quantum mechanics.

Transient Techniques in NMR of Author: Lynne Batchelder. Solid-state NMR (ssNMR) spectroscopy is a special type of nuclear magnetic resonance (NMR) spectroscopy, characterized by the presence of anisotropic (directionally dependent) interactions.

Compared to the more common solution NMR spectroscopy, ssNMR usually requires additional hardware for high-power radio-frequency irradiation and magic-angle spinning. Introduction to Solid State NMR Spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid-state nuclear magnetic resonance spectroscopy or undertaking research projects where solid-state NMR is likely to be a major investigative technique.

It will also serve as a practical introduction in industry, where the techniques can provide Author: Melinda J. Duer. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic book is divided into two parts.

The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods.

Resolution in 1 H NMR spectra of solids can be significantly enhanced with fast magic-angle spinning and high magnetic fields. A variable field and spinning speed study up to 25 T and 40 kHz shows that the homogeneous line broadening is inversely proportional to the product of Cited by: J.

Magn. Reson. 58, Gerstein B. and Dybowski C. () Transient Techniques in NMR in Solids. Academic Press, New York. Gerstein B. () High-resolution nmr in solids with strong homonuclear dipolar broadening: combined multiple-pulse deeoupling and magic angle spinning.

Phil. Trans. Soc. London A, Cited by:. Understanding the properties of pharmaceuticals in solid form is critical for drug development and efficacy. Over recent years, advances in solid-state nuclear magnetic resonance (NMR) spectroscopy have made the high-resolution analysis of these products a central method in the pharmaceutical industry.

The challenges of pharmaceutical polymorphs The majority of pharmaceuticals are produced .Hadamard NMR spectroscopy in solids. ID NMR techniques for separately obtaining individual powder patterns for chemically distinct nuclei using selective rf irra- diation and switching of the.Barth-Jan van Rossum: Solid-state NMR and proteins, a pictorial introduction Solid-state and solution NMR spectroscopy have many things in common Several concepts have been/will be discussed in the other lectures (spin precession, RF pulses, 2D experiments, chemical shift assignment, etc.) Æfeatures unique for solid-state NMR spectroscopyFile Size: 2MB.